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[�쑀湲고빀�꽦 �꽕怨� �봽濡쒖젥�듃] Synthesis of Trans-4-fluoro-L-proline

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자료설명
trans-4-fluoro-L-proline�쓽 �빀�꽦踰뺤쓣 �뿰援ы빐 蹂닿퀬, 媛��옣 ����졃�븯怨� 媛꾨떒�븯硫�, 移쒗솚寃쎌쟻�씤 猷⑦듃瑜� �넻�빐 �빀�꽦踰뺤쓣 �븣�븘蹂몃떎. 洹몃━怨� trans-4-fluoro-L-proline�쓽 �슜�룄瑜� 李얠븘蹂댁옄.
목차/차례
紐⑹감

�뀪. 紐� �쟻

�뀫. 議곗궗 �궡�슜

�뀬. �빀�꽦 scheme

�뀭. 寃� 濡�

蹂몃Ц�씪遺�
�슦�꽑 �쟻�쑝濡� �슦由� 議곕뒗 trans-4-fluoro-L-proline�쓽 �빀�꽦踰뺤쓣 �븣湲� �쐞�븯�뿬, �씠 臾쇱쭏�쓣 留뚮뱾湲� �쐞�븳 �빀�꽦踰� 以�, �깮媛곹빐 蹂� List瑜� �젙由� �빐 蹂댁븯�떎.

1) N�씠 �룷�븿�맂 5媛곹삎 �솕�빀臾�

2) F瑜� C�뿉 遺숈씠�뒗 諛⑸쾿

3) leaving group �룄�엯 諛⑸쾿

4) COOH湲곕�� 留뚮뱶�뒗 諛⑸쾿

5) Stereo Chemistry瑜� 議곗젅�븯�뒗 諛⑸쾿

6) 怨좊━ �솕�빀臾쇱쓣 �빀�꽦�븯�뒗 諛⑸쾿

7) �븘誘쇨린�뿉 ����븳 Protecting Group�뿉 愿��븳 議곗궗

8) 怨좊━ �솕�빀臾쇱뿉 �씠以� 寃고빀�쓣 �떒�씪 寃고빀�쑝濡� �솚�썝 �떆�궎�뒗 諛⑸쾿

�몺 Carbobenzyloxy

schematic:
Protection of amine with benzyl chloroformateCarboxybenzyl or Cbz or Z is an amine protecting group in organic synthesis. It is commonly used in peptide synthesis and is formed by reacting an amine with benzyl chloroformate and a weak base. It is used to protect amines from electrophiles. The protected amine can be deprotected by catalytic hydrogenation or treatment with HBr.

�몼 Di-tert-butyl dicarbonate

Di-tert-butyl dicarbonate is a reagent widely used in organic synthesis. This arbonate ester reacts with amines to give N-tert-butoxycarbonyl or so-called t-BOC derivatives. These derivatives do
본문/내용
[�쑀湲고빀�꽦�솕�븰 �꽕怨� project]

��쁔rans-4-fluoro-L-proline���
�쓽 �빀�꽦


3議�
200220550 �삤嫄댄솚
200421887 �뿀吏��샇
200521881 媛뺥슚吏�
200521895 源��쑄�쁺

Trans-4-fluoro-L-proline�쓽 �빀�꽦 ( 3議� )

�뀪. 紐� �쟻 :-trans-4-fluoro-L-proline�쓽 �빀�꽦踰뺤쓣 �뿰援ы빐 蹂닿퀬, 媛��옣 ����졃�븯怨� 媛꾨떒�븯硫�, 移쒗솚寃쎌쟻�씤 猷⑦듃瑜� �넻�빐 �빀�꽦踰뺤쓣 �븣�븘蹂몃떎. 洹몃━怨� trans-4-fluoro-L-proline�쓽 �슜�룄瑜� 李얠븘蹂댁옄.

Reference standard for trans-4-fluoro-L-proline

Product List

�뀫. 議곗궗 �궡�슜

�슦�꽑 �쟻�쑝濡� �슦由� 議곕뒗 trans-4-fluoro-L-proline�쓽 �빀�꽦踰뺤쓣 �븣湲� �쐞�븯�뿬, �씠 臾쇱쭏�쓣 留뚮뱾湲� �쐞�븳 �빀�꽦踰� 以�, �깮媛곹빐 蹂� List瑜� �젙由� �빐 蹂댁븯�떎.

1) N�씠 �룷�븿�맂 5媛곹삎 �솕�빀臾�
2) F瑜� C�뿉 遺숈씠�뒗 諛⑸쾿
3) leaving group �룄�엯 諛⑸쾿
4) COOH湲곕�� 留뚮뱶�뒗 諛⑸쾿
5) Stereo Chemistry瑜� 議곗젅�븯�뒗 諛⑸쾿
6) 怨좊━ �솕�빀臾쇱쓣 �빀�꽦�븯�뒗 諛⑸쾿
7) �븘誘쇨린�뿉 ����븳 Protecting Group�뿉 愿��븳 議곗궗
8) 怨좊━ �솕�빀臾쇱뿉 �씠以� 寃고빀�쓣 �떒�씪 寃고빀�쑝濡� �솚�썝 �떆�궎�뒗 諛⑸쾿

1. 異쒕컻臾쇱쭏濡� �깮媛곹븳 �솕�빀臾쇨낵 臾몄젣�젏

1) Pyrrole

-�깮媛곹빐 蹂� �젏: 2以� 寃고빀�씠 2媛쒓�� �엳湲� �븣臾몄뿉 COOH��� F瑜� 遺숈뿬二쇱뼱�빞 �븳�떎. �삉�븳 2以� 寃고빀�쓣 �솚�썝�븯�뒗 諛⑸쾿�쓣 �깮媛곹빐 蹂몃떎.

2) Methyl-2-pyrrolecarboxylate

-�깮媛곹빐 蹂� �젏: �씠 臾쇱쭏�뿉�뒗 C(O)OCH3媛� �엳�뒗�뜲 �씠 Functional Group�쓣 移대Ⅴ蹂듭떎湲곕줈 諛붽씀怨�, F瑜� 遺숈씠�뒗 �젏�쓣 �깮媛곹빐 蹂몃떎. �씠�븣 reduction�쓣 �떆�궎怨� C(O)OH濡쒖쓽 諛섏쓳�뿉�꽌 stereochemistry 議곗젅�씠 �옒�뱾 �벏 �븯�떎怨� �깮媛곷맂���(�깮�왂)
참고문헌
- Organic Chemistry / Oxford University Press, 2001J. Clayden, N. Greeves, S. Warren, P. Wothers
- The chemistry of pyrroles / Academic, Jones, R. Alan/Bean, Gerritt P.
- Selective fluorination in organic and bioorganic chemistry / American Chemical Society, Welch, John T
- �쑀湲고빀�꽦 / R. K. Mackie ; D. M. Smith ; R. A. Aitken ��� ; 怨쎌쁺�슦 �뿭
- �쑀湲고솕�븰 / Robert Thornton Morrison ; Robert Neilson Boyd怨듭��- Wikipedia , the free encyclopedia
- http://www.cem.msu.edu/~reusch/VirtTxtJml/alcohol1.htm


자료정보
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Regist : 2010-08-24
Update : 2017-04-01
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